Crystallization conditions |
Cell parameters |
Reference |
3.3M ammonium sulfate, pH 6.0
2.3M ammonium sulfate, 20mM KH2PO4, 1mM NH4OH, .1 mM EDTA, pH 6 |
P6222
a = b = 96.2 Å c = 168.0 Å |
1 5 |
16% PEG 6,000, 100mM Tris-HCl, 1mM EDTA, 1mM bME, 0.5% garamycin, pH 7.8, 2-4°C |
P212121 a = 86.3 Å b = 115.7 Å , c = 151.4 Å |
2 |
50-55% ammonium sulfate, pH 6.1-6.4, 2-3°C 2.3M ammonium sulfate, 100mM citrate, 5 mM EDTA, pH 6.0, 4°C |
P6222 a = b = 161.0 Å, c = 170.0 Å |
3 4,5 |
40-49% ammonium sulfate, 100mM TEA, 5% EDTA, pH 7.3 , 20°C (and with citrate buffer pH 5.5 |
P21 a = 164.5 Å, b = 57.3 Å, c = 85.0 Å beta=102.7° |
4 |
2M NaH2PO4, K2HPO4, pH 6.0-7.5. 50-55% ammonium sulfate, pH 6.1-6.4, 2-3°C. |
P6222 a = b = 163.5 Å, c = 335.0 Å |
6,3 |
45% ammonium sulfate, 0.1 M TEA-HCl , pH 7.4, 4°C
|
C2221 a = 377.0 Å, b = 130.3 Å, c = 80.0 Å |
7 |
20-40mM KH2PO4, 0-0.2 M ammonium sulfate, pH 3.5, 24°C
|
P213 a = b = c = 103.5 Å |
8 |
7% PEG 4,000, 30 mM Tris-HCl,2.5 mM Zn Cl2, pH 7.5
|
P6122 a = b = 78.4 Å, c = 290.6 Å |
9 |
20% MPEG 5,000, 200 mM imidazole malate, pH 6.0 |
P212121 a = 183.1 Å b = 61.4 Å , c = 43.9 Å |
This Work |
25% MPEG 2,000, 200 mM imidazole malate,250 mM LiCl, pH 5.8 and 3.8 mM 2-deoxyribose 5-phosphate |
P212121 a = 179.2 Å b = 60.5 Å , c = 49.1 Å |
This Work |